YU Shan-xin
Abstract
n-Butyl chloroacetate was synthesis from chloroacetic acid and n-butanol in the presence of p-toluene sulfuric acid. The yield of the ester could reach 93.3% under amount of substance ratio of chloroacetic acid, n-butanol and p-toluene sulfuric acid were 1:2.5:0.05, refluxing and water segregating for 90min.
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n-Butyl chloroacetate was synthesis from chloroacetic acid and n-butanol in the presence of p-toluene sulfuric acid. The yield of the ester could reach 93.3% under amount of substance ratio of chloroacetic acid, n-butanol and p-toluene sulfuric acid were 1:2.5:0.05, refluxing and water segregating for 90min.
Key concepts: Chloroacetic acid, Sulfuric acid, Toluene, Chemistry, Catalysis, Yield (engineering), Butanol, n-Butanol