2011•Shipin yu fajiao kejiRequires access

Determination of Fe,Mn,Cu and Zn Elements in Corn by Flame Atomic Absorption Spectrometry

LI Guo-lan

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Abstract

With HNO3~HClO4(4+1) wet indesgition method to pretreat samples,the contents of four elements Fe,Mn,Cu,Zn in Corn had been determinated by flame atomic absorption spectrometry.And the recovery rate of 97%~99% for Fe,95%~100% for Mn,95%~103% for Cu,100%~104% for Zn were obtained.The average rate was 95%~104%.RSD was 0.1%~0.9%.It was shown that the method was reliable for the test of precision and accuracy.

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What this paper is about

With HNO3~HClO4(4+1) wet indesgition method to pretreat samples,the contents of four elements Fe,Mn,Cu,Zn in Corn had been determinated by flame atomic absorption spectrometry.And the recovery rate of 97%~99% for Fe,95%~100% for Mn,95%~103% for Cu,100%~104% for Zn were obtained.The average rate was 95%~104%.RSD was 0.1%~0.9%.It was shown that the method was reliable for the test of precision and accuracy.

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Available abstract

With HNO3~HClO4(4+1) wet indesgition method to pretreat samples,the contents of four elements Fe,Mn,Cu,Zn in Corn had been determinated by flame atomic absorption spectrometry.And the recovery rate of 97%~99% for Fe,95%~100% for Mn,95%~103% for Cu,100%~104% for Zn were obtained.The average rate was 95%~104%.RSD was 0.1%~0.9%.It was shown that the method was reliable for the test of precision and accuracy.

Key concepts: Atomic absorption spectroscopy, Chemistry, Manganese, Zinc, Recovery rate, Analytical Chemistry (journal), Mass spectrometry, Absorption (acoustics)

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