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Determination of pyrethroid multi-residues in vegetables by high-performance liquid chromatography

Zenghong Xie

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Abstract

Simultaneous determination of five pyrethroid residues in vegetables including fenpropathrin,lambda-cyhalothrin,deltamethrin,fenvalerate and permethrin were performed by high performance liquid chromatography with florisil solid-phase extraction.Four kind samples with five pyrethroids were well detected under the optimized conditions.The recoveries for cabbage,cauliflower,carrot,and green pepper were 80.7%~106.2%,80.5%~102.0%,63.9%~109.3%,74.9%~109.0%,respectively.Their relative standard deviation(n=5) were less than 14.5%.

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What this paper is about

Simultaneous determination of five pyrethroid residues in vegetables including fenpropathrin,lambda-cyhalothrin,deltamethrin,fenvalerate and permethrin were performed by high performance liquid chromatography with florisil solid-phase extraction.Four kind samples with five pyrethroids were well detected under the optimized conditions.The recoveries for cabbage,cauliflower,carrot,and green pepper were 80.7%~106.2%,80.5%~102.0%,63.9%~109.3%,74.9%~109.0%,respectively.Their relative standard deviation(n=5) were less than 14.5%.

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Available abstract

Simultaneous determination of five pyrethroid residues in vegetables including fenpropathrin,lambda-cyhalothrin,deltamethrin,fenvalerate and permethrin were performed by high performance liquid chromatography with florisil solid-phase extraction.Four kind samples with five pyrethroids were well detected under the optimized conditions.The recoveries for cabbage,cauliflower,carrot,and green pepper were 80.7%~106.2%,80.5%~102.0%,63.9%~109.3%,74.9%~109.0%,respectively.Their relative standard deviation(n=5) were less than 14.5%.

Key concepts: Fenvalerate, Deltamethrin, Chemistry, Pyrethroid, Permethrin, Chromatography, Cyhalothrin, High-performance liquid chromatography

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