2009•Rengong jingti xuebaoRequires access

Hydrothermal Synthesis and Crystal Structure of a Supramolecular Network [Mn(phen)_2I_2]

LV Xiao-jiang

Abstract

A novel supramolecular network [Mn(phen)2I2] has been rationally designed and synthesized by hydrothermal method and the structure was characterized with elemental analysis,FT-IR spectrum and X-ray diffractometer. It crystallizes in the Triclinic,space group P1-,with a= 0.92705(19) nm,b= 1.0370 (2) nm,c=1.2775(3) nm,α=77.32(3) °,β=81.26(3) °,γ=70.30(3) °,V=1.1240(4) nm3,Z=2. In the title compound [Mn(phen)2I2],the separated unit cells are constructed into a novel supramolecular network by four types of C-H…I hydrogen-bonded and two kinds of π-π interactions.

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Key concepts: Triclinic crystal system, Diffractometer, Supramolecular chemistry, Crystallography, Hydrothermal synthesis, Materials science, Hydrothermal circulation, Crystal structure