1972•Journal of Synthetic Organic Chemistry JapanOpen access

The Reaction of Ethylene with 1, 1, 1, 3-Tetrachloropropane Initiated by Hexaethylphosphorous-triamide-Ferric Chloride

Toru Sato, A. KURITA, Manabu Senō, Teruzo Asahara

Abstract

The telomerization reaction of ethylene with 1, 1, 1, 3-tetrachloropropane initiated by hexaethylphosphorous-triamide-ferric chloride was investigated under various reaction conditions in a stainless steel autoclave. The reaction products were α, γ, γ, ω-tetrachloroalkane homologs which are the same as those from the reactions initiated by triethylphosphite-ferric salts ; 80-90 wt% of the products were the n=1 telomer (1, 3, 3, 5-tetrachloropentane)

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Key concepts: Telomerization, Ferric, Ethylene, Chemistry, Chloride, Autoclave, Polymer chemistry, Organic chemistry