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Microstructural Evolution and Mechanical Properties in Yb2O3–Fluxed Silicon Nitride Ceramics

Gang Feng Guo, Xiao Zhan Yang, Jian Bao Li, Hong Lin, Long Liang, Ming Sheng He, Tong Xu

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Abstract

Silicon nitride ceramics were fabricated with Yb2O3 as the sintering additive. The effects of the amount of Yb2O3 on the microstructure and the mechanical properties such as the flexural strength and the fracture toughness were investigated. Almost fully densified Si3N4 was obtained when only 4 wt% Yb2O3 was added. Both the flexural strength and the fracture toughness increased steadily with the Yb2O3 content. The transgranular fracture mode was observed in the specimen containing 4 wt% Yb2O3, however, the intergranular fracture mode was observed in the specimen containing 10 wt% Yb2O3.

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What this paper is about

Silicon nitride ceramics were fabricated with Yb2O3 as the sintering additive. The effects of the amount of Yb2O3 on the microstructure and the mechanical properties such as the flexural strength and the fracture toughness were investigated. Almost fully densified Si3N4 was obtained when only 4 wt% Yb2O3 was added. Both the flexural strength and the fracture toughness increased steadily with the Yb2O3 content. The transgranular fracture mode was observed in the specimen containing 4 wt% Yb2O3, however, the intergranular fracture mode was observed in the specimen containing 10 wt% Yb2O3.

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Available abstract

Silicon nitride ceramics were fabricated with Yb2O3 as the sintering additive. The effects of the amount of Yb2O3 on the microstructure and the mechanical properties such as the flexural strength and the fracture toughness were investigated. Almost fully densified Si3N4 was obtained when only 4 wt% Yb2O3 was added. Both the flexural strength and the fracture toughness increased steadily with the Yb2O3 content. The transgranular fracture mode was observed in the specimen containing 4 wt% Yb2O3, however, the intergranular fracture mode was observed in the specimen containing 10 wt% Yb2O3.

Key concepts: Materials science, Flexural strength, Transgranular fracture, Fracture toughness, Silicon nitride, Ceramic, Microstructure, Sintering

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