2005•Journal of the American Ceramic SocietyRequires access

Hydrothermal Synthesis of Anisotropic Monoclinic Zirconia Particles in the Presence of 1,12‐Diaminododecane

Fengxi Chen, Ziyi Zhong, Geok Joo Gan, Xiaojun Xu

Abstract

Anisotropic monoclinic zirconia particles (aspect ratio of 4–10) have been prepared upon hydrothermal processing of 1,12‐diaminododecane (DADD)‐hydrous zirconia gels at pH of 14 and at 230°C for 3 days. A biphasic growth model comprising melted DADD and the water/ethanol mixture is proposed to account for the generation of rod‐like morphology.

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Key concepts: Monoclinic crystal system, Cubic zirconia, Hydrothermal circulation, Materials science, Chemical engineering, Morphology (biology), Hydrothermal synthesis, Mineralogy