2008•Chinese Journal of ChemistryRequires access

A New Route to Preparations of Silyl Ethers by Reactions of Silyl Triflimides with Alcohol or Ether

Zi‐Long TANG

Abstract

Abstract A few of acyclic and cyclic silyl ethers were firstly synthesized in good yields by reactions of silyl triflimides with alcohol or ether. The corresponding silyl triflimides were easily produced by protodesilylation of phenyl or allyl silanes with HNTf2. All new compounds were characterized by 1H NMR, 13C NMR, MS, IR and HRMS.

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Key concepts: Chemistry, Silylation, Silyl ether, Silanes, Alcohol, Ether, Organic chemistry, Medicinal chemistry