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3:5‐dinitro‐4‐methyl‐benzazide as a reagent for the identification of phenols

Peter P. T. Sah

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Abstract

Abstract Thirty‐three crystalline urethanes were prepared by the condensation of the new reagent, 3:5‐dinitro‐4‐methyl‐benzazide, in boiling ligroin solution with various phenols. The very high yields of the 3:5‐dinitro‐4‐methylphenyl‐urethanes obtained from the reaction and the excellent properties of these derivatives, indicated that 3:5‐dinitro‐4‐methyl‐benzazide is an excellent micro‐reagent for the identification of phenols.

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Abstract Thirty‐three crystalline urethanes were prepared by the condensation of the new reagent, 3:5‐dinitro‐4‐methyl‐benzazide, in boiling ligroin solution with various phenols. The very high yields of the 3:5‐dinitro‐4‐methylphenyl‐urethanes obtained from the reaction and the excellent properties of these derivatives, indicated that 3:5‐dinitro‐4‐methyl‐benzazide is an excellent micro‐reagent for the identification of phenols.

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Available abstract

Abstract Thirty‐three crystalline urethanes were prepared by the condensation of the new reagent, 3:5‐dinitro‐4‐methyl‐benzazide, in boiling ligroin solution with various phenols. The very high yields of the 3:5‐dinitro‐4‐methylphenyl‐urethanes obtained from the reaction and the excellent properties of these derivatives, indicated that 3:5‐dinitro‐4‐methyl‐benzazide is an excellent micro‐reagent for the identification of phenols.

Key concepts: Reagent, Phenols, Boiling, Condensation, Chemistry, Phenol, Organic chemistry, Condensation reaction

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