1975•Journal of the Chemical Society Perkin Transactions 2Requires access

Crystal structure and absolute configuration of lycopodine hydrochloride

Mazhar Ul Haque, Donald B. Rogers

Abstract

Crystals of the title compound are orthorhombic, space group P212121, a= 7·606(1), b= 9·540(1),c= 21.371(1)Å, Z= 4. The structure was solved from diffractometer data by Patterson and heavy-atom methods and refined by full-matrix least-squares to R 0·050 for 1687 independent reflexions. The results confirm the chirality (I) earlier deduced from chemical work and a positive Cotton effect.

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Key concepts: Orthorhombic crystal system, Diffractometer, Absolute configuration, Crystallography, Chemistry, Chirality (physics), Atom (system on chip), Crystal structure