1996Analytical LettersRequires access

Determination of Enantiomer Excess of Asymmetric Hydroesterification Reaction by Hplc using A Cellulose Tribenzoate Chiral Column

Jingguo Hou, Hongying Zhou, Zhiqiang Zhou, Liren Chen, Qingyu Ou

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Abstract

The preparation of cellulose tribenzoate (CTB) chiral stationary phases coated on a small-particle (5 μ m, 120A°) spherical silica support, according to a process that is reported, is presented. The products of asymmetric hydroesterification of norbornene are resolved on the cellulose tribenzoate chiral stationary phases.

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What this paper is about

The preparation of cellulose tribenzoate (CTB) chiral stationary phases coated on a small-particle (5 μ m, 120A°) spherical silica support, according to a process that is reported, is presented. The products of asymmetric hydroesterification of norbornene are resolved on the cellulose tribenzoate chiral stationary phases.

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Available abstract

The preparation of cellulose tribenzoate (CTB) chiral stationary phases coated on a small-particle (5 μ m, 120A°) spherical silica support, according to a process that is reported, is presented. The products of asymmetric hydroesterification of norbornene are resolved on the cellulose tribenzoate chiral stationary phases.

Key concepts: Chemistry, Enantiomer, Chromatography, Cellulose, Chiral column chromatography, High-performance liquid chromatography, Chiral stationary phase, Enantiomeric excess

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