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2010•Zeitschrift für anorganische und allgemeine ChemieRequires access

Solvothermal Synthesis, Crystal Structures, and Magnetic Properties of Two Organically Templated Iron Sulfates with Chain Structures

Ling Ma, Dan Liu, Yan Xing, Xianchun Liu, Gaijuan Li

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Abstract

Abstract Two new one‐dimensional (1D) organically templated iron(III) sulfates [C2NH8]3 [Fe3(μ3‐O)2(SO4)4] (1) and [C2N2H10][C2NH7]0.5[FeF(SO4)2] (2) were synthesized under solvothermal conditions and characterized by single‐crystal X‐ray diffraction, powder X‐ray diffraction (XRD), FT‐IR spectroscopy, elemental analyses, ICP analyses, and thermogravimetric analyses. Single‐crystal structure analysis reveals that both compounds show linear‐chain structures, involving FeO6 (FeF2O4) octahedra and SO4 tetrahedra. The magnetic properties of the two compounds have also been investigated.

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Abstract Two new one‐dimensional (1D) organically templated iron(III) sulfates [C2NH8]3 [Fe3(μ3‐O)2(SO4)4] (1) and [C2N2H10][C2NH7]0.5[FeF(SO4)2] (2) were synthesized under solvothermal conditions and characterized by single‐crystal X‐ray diffraction, powder X‐ray diffraction (XRD), FT‐IR spectroscopy, elemental analyses, ICP analyses, and thermogravimetric analyses. Single‐crystal structure analysis reveals that both compounds show linear‐chain structures, involving FeO6 (FeF2O4) octahedra and SO4 tetrahedra. The magnetic properties of the two compounds have also been investigated.

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Available abstract

Abstract Two new one‐dimensional (1D) organically templated iron(III) sulfates [C2NH8]3 [Fe3(μ3‐O)2(SO4)4] (1) and [C2N2H10][C2NH7]0.5[FeF(SO4)2] (2) were synthesized under solvothermal conditions and characterized by single‐crystal X‐ray diffraction, powder X‐ray diffraction (XRD), FT‐IR spectroscopy, elemental analyses, ICP analyses, and thermogravimetric analyses. Single‐crystal structure analysis reveals that both compounds show linear‐chain structures, involving FeO6 (FeF2O4) octahedra and SO4 tetrahedra. The magnetic properties of the two compounds have also been investigated.

Key concepts: Thermogravimetric analysis, Crystallography, Octahedron, Crystal structure, Solvothermal synthesis, Powder diffraction, Elemental analysis, Single crystal

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Solvothermal Synthesis, Crystal Structures, and Magnetic Properties of Two Organically Templated Iron Sulfates with Chain Structures — Research Paper | ScholarLens