2009•eXPRESS Polymer LettersOpen access

Effect of electron beam irradiation and poly(vinylpyrrolidone) addition on mechanical properties of polycaprolactone with empty fruit bunch fibre (OPEFB) composite

Nor Azowa Ibrahim, Siti Nur Afifi Ahmad, Wan Md Zin Wan Yunus, Khairul Zaman Mohd Dahlan

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Abstract

Biodegradable composites or green composites were prepared by melt blending technique using polycaprolactone and oil palm empty fruit bunch fibre (OPEFB).Since OPEFB is not compatible with PCL a binder, poly(vinyl pyrrolidone), (PVP) was used to improve the interaction between PCL and OPEFB.The composites produced were irradiated using electron beam to improve the mechanical properties.The tensile, flexural and impact strengths of PCL/OPEFB composites were improved by addition of 1% by weight of PVP and irradiated with 10 kGy of electron beam.The FTIR spectra indicate a slight increase of frequencies at C=O peaks from 1730 to 1732 cm -1 after irradiation indicates some interaction between C=O and O-H.The surface morphology of the facture surface obtained from tensile test shows no fibre pull out indicating good adhesion between the OPEFB and PCL after addition of PVP.

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Biodegradable composites or green composites were prepared by melt blending technique using polycaprolactone and oil palm empty fruit bunch fibre (OPEFB).Since OPEFB is not compatible with PCL a binder, poly(vinyl pyrrolidone), (PVP) was used to improve the interaction between PCL and OPEFB.The composites produced were irradiated using electron beam to improve the mechanical properties.The tensile, flexural and impact strengths of PCL/OPEFB composites were improved by addition of 1% by weight of PVP and irradiated with 10 kGy of electron beam.The FTIR spectra indicate a slight increase of frequencies at C=O peaks from 1730 to 1732 cm -1 after irradiation indicates some interaction between C=O and O-H.The surface morphology of the facture surface obtained from tensile test shows no fibre pull out indicating good adhesion between the OPEFB and PCL after addition of PVP.

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Available abstract

Biodegradable composites or green composites were prepared by melt blending technique using polycaprolactone and oil palm empty fruit bunch fibre (OPEFB).Since OPEFB is not compatible with PCL a binder, poly(vinyl pyrrolidone), (PVP) was used to improve the interaction between PCL and OPEFB.The composites produced were irradiated using electron beam to improve the mechanical properties.The tensile, flexural and impact strengths of PCL/OPEFB composites were improved by addition of 1% by weight of PVP and irradiated with 10 kGy of electron beam.The FTIR spectra indicate a slight increase of frequencies at C=O peaks from 1730 to 1732 cm -1 after irradiation indicates some interaction between C=O and O-H.The surface morphology of the facture surface obtained from tensile test shows no fibre pull out indicating good adhesion between the OPEFB and PCL after addition of PVP.

Key concepts: Polycaprolactone, Materials science, Composite number, Irradiation, Composite material, Cathode ray, Electron, Polymer

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Effect of electron beam irradiation and poly(vinylpyrrolidone) addition on mechanical properties of polycaprolactone with empty fruit bunch fibre (OPEFB) composite — Research Paper | ScholarLens