1968The AnalystRequires access

A rapid procedure for the identification of organochlorine pesticides in blood and tissues

C Eliakis, A. Coutselinis, E Eliakis

Open publisher page 7 citations

Abstract

A method is described for the rapid identification of chlorinated insecticides, such as aldrin, dieldrin, op′-DDT and pp′-DDT, in tissues and blood, without the necessity for a previous clean-up procedure of the extracts made from them.Two-dimensional thin-layer chromatography was used for this purpose. The plates were developed in hexane for one dimension and in cyclohexane for the other, and were sprayed with a solution of 0·5 per cent. silver nitrate in ethanol before exposure to germicidal ultraviolet light. The sensitivity of this method is 0·5 µg, which is suitable for routine analysis.

About this research paper

What this paper is about

A method is described for the rapid identification of chlorinated insecticides, such as aldrin, dieldrin, op′-DDT and pp′-DDT, in tissues and blood, without the necessity for a previous clean-up procedure of the extracts made from them.Two-dimensional thin-layer chromatography was used for this purpose. The plates were developed in hexane for one dimension and in cyclohexane for the other, and were sprayed with a solution of 0·5 per cent. silver nitrate in ethanol before exposure to germicidal ultraviolet light. The sensitivity of this method is 0·5 µg, which is suitable for routine analysis.

Why it matters

OpenAlex reports 7 citations for this work. Citation counts describe recorded attention and do not establish research quality.

Key contribution

A contribution statement is not available in the OpenAlex record.

Method / approach

Method details are not available in the OpenAlex metadata.

Main findings

Findings are not separately available in the OpenAlex metadata.

Limitations

Limitations are not available in the OpenAlex metadata.

Applications

Application details are not available in the OpenAlex metadata.

Available abstract

A method is described for the rapid identification of chlorinated insecticides, such as aldrin, dieldrin, op′-DDT and pp′-DDT, in tissues and blood, without the necessity for a previous clean-up procedure of the extracts made from them.Two-dimensional thin-layer chromatography was used for this purpose. The plates were developed in hexane for one dimension and in cyclohexane for the other, and were sprayed with a solution of 0·5 per cent. silver nitrate in ethanol before exposure to germicidal ultraviolet light. The sensitivity of this method is 0·5 µg, which is suitable for routine analysis.

Key concepts: Dieldrin, Aldrin, Organochlorine pesticide, Pesticide, Environmental chemistry, Chemistry, Chromatography, Identification (biology)

Related papers

Back to paper searchBrowse research topicsOriginal source
A rapid procedure for the identification of organochlorine pesticides in blood and tissues — Research Paper | ScholarLens