The Synthesis of Mesoporous Molecular Sieve MCM-41 in Glycerol System
Xiumei Tai, Hongxia Wang, Jian Zhang, Xiuqi Shi
Abstract
Xiumei Tai, Hongxia Wang, Jian Zhang, Xiuqi Shi
Abstract
Abstract An efficient method for mesoporous molecular sieve MCM-41 was introduced in this report. In EDA/TEOS/CTAB/glycerol system, mesoporous molecular sieve MCM-41 has been synthesized at room temperature and under hydrothermal condition, respectively, characterized by X-ray power diffraction and N2 adsorption. Compared with the samples synthesized under hydrothermal condition, the samples synthesized at room temperature have better order, larger pore diameter and narrower pore diameter distribution.
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Abstract An efficient method for mesoporous molecular sieve MCM-41 was introduced in this report. In EDA/TEOS/CTAB/glycerol system, mesoporous molecular sieve MCM-41 has been synthesized at room temperature and under hydrothermal condition, respectively, characterized by X-ray power diffraction and N2 adsorption. Compared with the samples synthesized under hydrothermal condition, the samples synthesized at room temperature have better order, larger pore diameter and narrower pore diameter distribution.
Key concepts: Molecular sieve, Mesoporous material, MCM-41, Chemistry, Hydrothermal circulation, Glycerol, Adsorption, Chemical engineering