2010Journal of the Ceramic Society of JapanOpen access

Fine-grained AlN ceramics from nanopowder by spark plasma sintering

Toshiyuki Nishimura, Keisuke SEKINE, Yoshinobu Yamamoto, Naoto Hirosaki, Takamasa Ishigaki

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Abstract

Aluminum nitride nanopowder was fabricated from transition alumina nanopowder by gas reduction–nitridation method. It was sintered by spark plasma sintering with 1 wt % Ca3Al2O6 as a sintering additive in nitrogen. The nanopowder with Ca3Al2O6 was densified up to 3.16 Mg/m3 of density at 1450°C, restraining grain growth. The nanopowder without additive was densified at 1550°C. The sintering temperature for dense aluminum nitride ceramic could be reduced by 1 wt % Ca3Al2O6 as a sintering additive.

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Aluminum nitride nanopowder was fabricated from transition alumina nanopowder by gas reduction–nitridation method. It was sintered by spark plasma sintering with 1 wt % Ca3Al2O6 as a sintering additive in nitrogen. The nanopowder with Ca3Al2O6 was densified up to 3.16 Mg/m3 of density at 1450°C, restraining grain growth. The nanopowder without additive was densified at 1550°C. The sintering temperature for dense aluminum nitride ceramic could be reduced by 1 wt % Ca3Al2O6 as a sintering additive.

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Available abstract

Aluminum nitride nanopowder was fabricated from transition alumina nanopowder by gas reduction–nitridation method. It was sintered by spark plasma sintering with 1 wt % Ca3Al2O6 as a sintering additive in nitrogen. The nanopowder with Ca3Al2O6 was densified up to 3.16 Mg/m3 of density at 1450°C, restraining grain growth. The nanopowder without additive was densified at 1550°C. The sintering temperature for dense aluminum nitride ceramic could be reduced by 1 wt % Ca3Al2O6 as a sintering additive.

Key concepts: Spark plasma sintering, Materials science, Sintering, Ceramic, Nitride, Grain growth, Metallurgy, Nanoparticle

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