Thermal outgassing behavior and photoemission studies of Haynes Alloy 214
Pramod K. Sharma, Gregory S. Hickey
Abstract
Pramod K. Sharma, Gregory S. Hickey
Abstract
Processing of many materials at high temperatures requires a high purity environment. The outgassing from hot surfaces of the processing chamber or the heating elements is a potential problem. The total amount of outgassing as well as the time- and temperature- dependent outgassing rates are important. The outgassing from Haynes Alloy 214 has been studied experimentally under a vacuum in the temperature range from room temperature to 600 °C. In addition to the outgassing rates, the composition of the outgassed species was determined through mass spectrometric analysis. Alloy surface composition was determined by x-ray photoelectron spectroscopy. Changes in surface composition before and after heating can be accounted for by the outgassed species.
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Processing of many materials at high temperatures requires a high purity environment. The outgassing from hot surfaces of the processing chamber or the heating elements is a potential problem. The total amount of outgassing as well as the time- and temperature- dependent outgassing rates are important. The outgassing from Haynes Alloy 214 has been studied experimentally under a vacuum in the temperature range from room temperature to 600 °C. In addition to the outgassing rates, the composition of the outgassed species was determined through mass spectrometric analysis. Alloy surface composition was determined by x-ray photoelectron spectroscopy. Changes in surface composition before and after heating can be accounted for by the outgassed species.
Key concepts: Outgassing, X-ray photoelectron spectroscopy, Alloy, Materials science, Analytical Chemistry (journal), Chemistry, Metallurgy, Chemical engineering