2009Geophysical Journal InternationalOpen access

Measuring remanence anisotropy of hematite in red beds: anisotropy of high-field isothermal remanence magnetization (hf-AIR)

Dario Bilardello, Kenneth P. Kodama

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Abstract

The potential of using high-field anisotropy of isothermal remanence magnetization (hf-AIR) measurements for determining the origin of natural remanent magnetization in red beds and for identifying and correcting possible red-bed inclination shallowing was investigated for specimens of the Carboniferous Shepody Formation of New Brunswick and Nova Scotia, Canada.The technique makes it possible for a typical paleomagnetic laboratory to measure the remanence anisotropy of high-coercivity hematite.High-field (hf) AIR was used in conjunction with 100 mT alternating field (af) and 120 • C thermal demagnetization to separate the contribution of hematite to the remanence anisotropy from that of magnetite/maghemite and goethite, respectively.A 5-T impulse DC magnetic field was used for the hf-AIR to reset the magnetic moment of high-coercivity hematite so that demagnetization between AIR orientations was not necessary.The ability of a 5-T field to reset the magnetization was tested by generating an isothermal remanent magnetization acquisition curve for hematite by using impulse DC magnetic fields up to 5 T in one orientation and followed by applying a field in the opposite direction at each step.Each field application was treated by 120 • C heating and 100 mT af demagnetization before measurement.At 5T, the difference between the magnetizations applied in opposite directions disappeared indicating that no magnetic memory persisted at this field strength.We performed a validity and reproducibility test of our hf-AIR measurement technique by measuring three specimens multiple times along two orthogonal coordinate systems.The method yielded highly reproducible results and, on rotating the specimen's coordinates, the fabric rotated by 90 • as expected, showing that it is not an artifact of the technique.We also measured hf-AIR on samples that had previously been chemically demagnetized in 3N HCl to remove the secondary, chemically grown pigmentary hematite.The hf-AIR fabric of leached samples is similar to that of untreated samples, but shows a better-defined magnetic lineation and imbrication.We interpret the fabric observed for the Shepody Formation to be a compactional fabric that has been reoriented by strain during folding following a flexural-slip model.

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The potential of using high-field anisotropy of isothermal remanence magnetization (hf-AIR) measurements for determining the origin of natural remanent magnetization in red beds and for identifying and correcting possible red-bed inclination shallowing was investigated for specimens of the Carboniferous Shepody Formation of New Brunswick and Nova Scotia, Canada.The technique makes it possible for a typical paleomagnetic laboratory to measure the remanence anisotropy of high-coercivity hematite.High-field (hf) AIR was used in conjunction with 100 mT alternating field (af) and 120 • C thermal demagnetization to separate the contribution of hematite to the remanence anisotropy from that of magnetite/maghemite and goethite, respectively.A 5-T impulse DC magnetic field was used for the hf-AIR to reset the magnetic moment of high-coercivity hematite so that demagnetization between AIR orientations was not necessary.The ability of a 5-T field to reset the magnetization was tested by generating an isothermal remanent magnetization acquisition curve for hematite by using impulse DC magnetic fields up to 5 T in one orientation and followed by applying a field in the opposite direction at each step.Each field application was treated by 120 • C heating and 100 mT af demagnetization before measurement.At 5T, the difference between the magnetizations applied in opposite directions disappeared indicating that no magnetic memory persisted at this field strength.We performed a validity and reproducibility test of our hf-AIR measurement technique by measuring three specimens multiple times along two orthogonal coordinate systems.The method yielded highly reproducible results and, on rotating the specimen's coordinates, the fabric rotated by 90 • as expected, showing that it is not an artifact of the technique.We also measured hf-AIR on samples that had previously been chemically demagnetized in 3N HCl to remove the secondary, chemically grown pigmentary hematite.The hf-AIR fabric of leached samples is similar to that of untreated samples, but shows a better-defined magnetic lineation and imbrication.We interpret the fabric observed for the Shepody Formation to be a compactional fabric that has been reoriented by strain during folding following a flexural-slip model.

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Available abstract

The potential of using high-field anisotropy of isothermal remanence magnetization (hf-AIR) measurements for determining the origin of natural remanent magnetization in red beds and for identifying and correcting possible red-bed inclination shallowing was investigated for specimens of the Carboniferous Shepody Formation of New Brunswick and Nova Scotia, Canada.The technique makes it possible for a typical paleomagnetic laboratory to measure the remanence anisotropy of high-coercivity hematite.High-field (hf) AIR was used in conjunction with 100 mT alternating field (af) and 120 • C thermal demagnetization to separate the contribution of hematite to the remanence anisotropy from that of magnetite/maghemite and goethite, respectively.A 5-T impulse DC magnetic field was used for the hf-AIR to reset the magnetic moment of high-coercivity hematite so that demagnetization between AIR orientations was not necessary.The ability of a 5-T field to reset the magnetization was tested by generating an isothermal remanent magnetization acquisition curve for hematite by using impulse DC magnetic fields up to 5 T in one orientation and followed by applying a field in the opposite direction at each step.Each field application was treated by 120 • C heating and 100 mT af demagnetization before measurement.At 5T, the difference between the magnetizations applied in opposite directions disappeared indicating that no magnetic memory persisted at this field strength.We performed a validity and reproducibility test of our hf-AIR measurement technique by measuring three specimens multiple times along two orthogonal coordinate systems.The method yielded highly reproducible results and, on rotating the specimen's coordinates, the fabric rotated by 90 • as expected, showing that it is not an artifact of the technique.We also measured hf-AIR on samples that had previously been chemically demagnetized in 3N HCl to remove the secondary, chemically grown pigmentary hematite.The hf-AIR fabric of leached samples is similar to that of untreated samples, but shows a better-defined magnetic lineation and imbrication.We interpret the fabric observed for the Shepody Formation to be a compactional fabric that has been reoriented by strain during folding following a flexural-slip model.

Key concepts: Remanence, Natural remanent magnetization, Anisotropy, Hematite, Stoner–Wohlfarth model, Paleomagnetism, Geology, Coercivity

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