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1990•Magnetic Resonance in ChemistryRequires access

HMQC‐NOESY: Application to a polynuclear aromatic at natural abundance

Ronald Ronald, C. Crouch, C. Webster Andrews, Gary E. Martin, Jiann‐Kuan Luo, Raymond N. Castle

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Abstract

Abstract Orientation of proton spin systems relative to one another in polynuclear aromatics through the use of 1H homo‐nuclear nuclear Overhauser effects (NOE) detected by heteronuclear multiple quantum correlation (HMQC‐NOESY) at natural abundance is reported. The experiment was explored as a potential alternative for problems in which a solution cannot be obtained by more conventional methods. Optimization of the HMQC‐NOESY experiment is discussed.

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What this paper is about

Abstract Orientation of proton spin systems relative to one another in polynuclear aromatics through the use of 1H homo‐nuclear nuclear Overhauser effects (NOE) detected by heteronuclear multiple quantum correlation (HMQC‐NOESY) at natural abundance is reported. The experiment was explored as a potential alternative for problems in which a solution cannot be obtained by more conventional methods. Optimization of the HMQC‐NOESY experiment is discussed.

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Available abstract

Abstract Orientation of proton spin systems relative to one another in polynuclear aromatics through the use of 1H homo‐nuclear nuclear Overhauser effects (NOE) detected by heteronuclear multiple quantum correlation (HMQC‐NOESY) at natural abundance is reported. The experiment was explored as a potential alternative for problems in which a solution cannot be obtained by more conventional methods. Optimization of the HMQC‐NOESY experiment is discussed.

Key concepts: Heteronuclear molecule, Chemistry, Nuclear Overhauser effect, Two-dimensional nuclear magnetic resonance spectroscopy, Proton, Nuclear magnetic resonance spectroscopy, Stereochemistry, Nuclear magnetic resonance

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