Analysis of Volatile Compounds from Oriental Melons (Cucumis melo L.) Using Headspace SPME Coupled with GC-MS
Yu Yang, Ze Yuan Yu, Ya Qin Xu, Shao Qin
Abstract
Yu Yang, Ze Yuan Yu, Ya Qin Xu, Shao Qin
Abstract
The quantitative distribution of volatile compounds in the different oriental melon varieties and in the different parts of oriental melon was investigated. Volatile compounds were extracted by solid-phase microextraction (SPME) and analysed by gas chromatography-mass spectrometry (GC-MS). Fifty-four compounds were identified including 33 esters, 3 thioesters, 7 aldehydes, 8 alcohols, 1 acid, 1 ketone and 1 phenol, among which esters were found to be the major constituents in ripe oriental melon. The results showed that ethyl acetate, sulfur-containing esters and compounds containing a straight nine-carbon chain were present at high concentrations in oriental melons, particularly acetic acid phenylmethyl ester. The majority of ester compounds of oriental melon decreased and the aldehyde compounds increased after storage at -20 °C and the distribution of volatiles was also found to be different in the umbilicus, middle and pedicel of an oriental melon Qitian 1 according to their carbon chain length and quantity.
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The quantitative distribution of volatile compounds in the different oriental melon varieties and in the different parts of oriental melon was investigated. Volatile compounds were extracted by solid-phase microextraction (SPME) and analysed by gas chromatography-mass spectrometry (GC-MS). Fifty-four compounds were identified including 33 esters, 3 thioesters, 7 aldehydes, 8 alcohols, 1 acid, 1 ketone and 1 phenol, among which esters were found to be the major constituents in ripe oriental melon. The results showed that ethyl acetate, sulfur-containing esters and compounds containing a straight nine-carbon chain were present at high concentrations in oriental melons, particularly acetic acid phenylmethyl ester. The majority of ester compounds of oriental melon decreased and the aldehyde compounds increased after storage at -20 °C and the distribution of volatiles was also found to be different in the umbilicus, middle and pedicel of an oriental melon Qitian 1 according to their carbon chain length and quantity.
Key concepts: Chemistry, Melon, Solid-phase microextraction, Acetic acid, Gas chromatography–mass spectrometry, Chromatography, Aldehyde, Phenol