1968Journal of Physics E Scientific InstrumentsOpen access

An inexpensive, bakeable quadrupole mass spectrometer

David Smith, P R Cromey

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Abstract

The design, construction and operation of a simple and inexpensive quadrupole mass spectrometer is described. The spectrometer covers the mass range 1 to 100 A.U. and the resolving power of the instrument is variable up to about 100. The use of a machinable ceramic material to support the electrodes enables the spectrometer to be baked for outgassing purposes and to be operated over a wide range of temperature. Although the spectrometer described is tuned manually, the instrument has been used in conjunction with a sawtooth waveform generator to obtain an automatic mass scan with a scan period of about 0·1 s.

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The design, construction and operation of a simple and inexpensive quadrupole mass spectrometer is described. The spectrometer covers the mass range 1 to 100 A.U. and the resolving power of the instrument is variable up to about 100. The use of a machinable ceramic material to support the electrodes enables the spectrometer to be baked for outgassing purposes and to be operated over a wide range of temperature. Although the spectrometer described is tuned manually, the instrument has been used in conjunction with a sawtooth waveform generator to obtain an automatic mass scan with a scan period of about 0·1 s.

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Available abstract

The design, construction and operation of a simple and inexpensive quadrupole mass spectrometer is described. The spectrometer covers the mass range 1 to 100 A.U. and the resolving power of the instrument is variable up to about 100. The use of a machinable ceramic material to support the electrodes enables the spectrometer to be baked for outgassing purposes and to be operated over a wide range of temperature. Although the spectrometer described is tuned manually, the instrument has been used in conjunction with a sawtooth waveform generator to obtain an automatic mass scan with a scan period of about 0·1 s.

Key concepts: Quadrupole mass analyzer, Spectrometer, Hybrid mass spectrometer, Mass spectrometry, Outgassing, Triple quadrupole mass spectrometer, Sawtooth wave, Materials science

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