Determination of ascorbyl 6-palmitate in food matrices by amperometric flow injection analysis
Susanna Buratti, Maria Stella Cosio, S. Benedetti, Saverio Mannino
Abstract
Susanna Buratti, Maria Stella Cosio, S. Benedetti, Saverio Mannino
Abstract
In this paper a rapid method based on a FIA (flow injection analysis) system with amperometric detection for the evaluation of ascorbyl 6-palmitate in foods is described. The selectivity of the proposed method is related to the low anodic potential applied to the working glassy carbon electrode (+0.1 V vs. Ag/AgCl) that leaves out interferences from ascorbic acid and phenolic compounds. By flow injection analysis, under optimised conditions, the calibration curve was linear in the range 0-20 mg l(-1) and the detection limit was 0.2 mg l(-1).
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In this paper a rapid method based on a FIA (flow injection analysis) system with amperometric detection for the evaluation of ascorbyl 6-palmitate in foods is described. The selectivity of the proposed method is related to the low anodic potential applied to the working glassy carbon electrode (+0.1 V vs. Ag/AgCl) that leaves out interferences from ascorbic acid and phenolic compounds. By flow injection analysis, under optimised conditions, the calibration curve was linear in the range 0-20 mg l(-1) and the detection limit was 0.2 mg l(-1).
Key concepts: Amperometry, Flow injection analysis, Ascorbic acid, Detection limit, Chemistry, Calibration curve, Linear range, Chromatography