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A diamond-anvil cell for single-crystal x-ray diffraction studies to pressures in excess of 10 GPa

David R. Allan, R. Miletich, Ross John Angel

Open publisher page 100 citations

Abstract

A new diamond-anvil cell for single-crystal x-ray diffraction structural studies is presented. By including a simple mechanism for adjusting the parallelism of the opposing diamond culets, the stability of the gasket is maintained to higher pressures than was achieved in earlier cells of a similar two-platen design. Equipped with 600 μm culet diamond anvils, the cell has been tested to a pressure of 25 GPa and has been used successfully for equation-of-state measurements and crystal structure determinations to 10 GPa.

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What this paper is about

A new diamond-anvil cell for single-crystal x-ray diffraction structural studies is presented. By including a simple mechanism for adjusting the parallelism of the opposing diamond culets, the stability of the gasket is maintained to higher pressures than was achieved in earlier cells of a similar two-platen design. Equipped with 600 μm culet diamond anvils, the cell has been tested to a pressure of 25 GPa and has been used successfully for equation-of-state measurements and crystal structure determinations to 10 GPa.

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Available abstract

A new diamond-anvil cell for single-crystal x-ray diffraction structural studies is presented. By including a simple mechanism for adjusting the parallelism of the opposing diamond culets, the stability of the gasket is maintained to higher pressures than was achieved in earlier cells of a similar two-platen design. Equipped with 600 μm culet diamond anvils, the cell has been tested to a pressure of 25 GPa and has been used successfully for equation-of-state measurements and crystal structure determinations to 10 GPa.

Key concepts: Diamond anvil cell, Diffraction, Diamond, Gasket, Materials science, X-ray crystallography, Single crystal, Equation of state

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