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Copolymerization of 4,4′-divinyl benzoyl peroxide with methyl methacylate and grafting of butyl acrylates onto the copolymers

Zhiang Li, Qiangguo Du, Xuezhen Shi, Fenggang Tao, Quanrui Wang, Graham Swift, Shuguang Wu

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Abstract

A peroxide monomer, 4,4′-divinyl benzoyl peroxide (DVBPO), was synthesized. Bulk copolymerization of DVBPO with methyl methacrylate (MMA) was initiated by di(2-ethyl hexyl)peroxy carbonate (EHP). DSC curves and the appearance of crosslinking of the product showed that DVBPO can copolymerize with MMA. The grafting copolymerization of butyl acrylate (BA) onto the copolymer was performed. The grafting efficiency (GE), determined by Soxhlet extraction, was high.

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What this paper is about

A peroxide monomer, 4,4′-divinyl benzoyl peroxide (DVBPO), was synthesized. Bulk copolymerization of DVBPO with methyl methacrylate (MMA) was initiated by di(2-ethyl hexyl)peroxy carbonate (EHP). DSC curves and the appearance of crosslinking of the product showed that DVBPO can copolymerize with MMA. The grafting copolymerization of butyl acrylate (BA) onto the copolymer was performed. The grafting efficiency (GE), determined by Soxhlet extraction, was high.

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Available abstract

A peroxide monomer, 4,4′-divinyl benzoyl peroxide (DVBPO), was synthesized. Bulk copolymerization of DVBPO with methyl methacrylate (MMA) was initiated by di(2-ethyl hexyl)peroxy carbonate (EHP). DSC curves and the appearance of crosslinking of the product showed that DVBPO can copolymerize with MMA. The grafting copolymerization of butyl acrylate (BA) onto the copolymer was performed. The grafting efficiency (GE), determined by Soxhlet extraction, was high.

Key concepts: Benzoyl peroxide, Copolymer, Grafting, Methyl methacrylate, Polymer chemistry, Monomer, Peroxide, Methyl acrylate

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