1983•Journal of the Chemical Society Chemical CommunicationsRequires access

N,N-bis-(1-aryl-3-methyltriazen-3-ylmethyl)methylamines (1,9-diaryl-3,5,7-trimethyl-1,2,3,5,7,8,9-hepta-azanona-1,8-dienes): novel coupling products from the reaction of arenediazonium ions with methylamine and formaldehyde

Ronald J. LaFrance, York Tang, Keith Vaughan, Donald L. Hooper

Abstract

The reaction of arenediazonium ions with aqueous formaldehyde–methylamine solution affords mixtures of the 3-hydroxymethyltriazenes, ArNNN(Me)CH2OH, and the previously unreported bis(triazenylmethyl)methyl-amines, ArNNN(Me)CH2N(Me)CH2N(Me)NNAr.

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Key concepts: Methylamines, Methylamine, Chemistry, Formaldehyde, Aryl, Aqueous solution, Ion, Medicinal chemistry