1969•Journal of the Chemical Society D Chemical CommunicationsRequires access

Direct nuclear magnetic resonance observation of Me2Mg and MeMgBr in a diethyl ether solution of methylmagnesium bromide

E. C. Ashby, George E. Parris, Frank E. Walker

Abstract

100 MHz n.m.r. spectra of dimethylmagnesium, methylmagnesium bromide, and a mixture of dimethylmagnesium and methylmagnesium bromide from +30 to –105° reveal the presence of MeMgBr and Me2Mg species in diethyl ether solution of the Grignard reagent.

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Key concepts: Chemistry, Bromide, Diethyl ether, Reagent, Ether, Spectral line, Organic chemistry, Physics