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2004•Acta Crystallographica Section C Crystal Structure CommunicationsOpen access

Partially oxidized {2-[(benzoylmethylene)diphenyl-λ5-phosphino]ethyl}diphenylphosphine as a monohydrate

E. Mothi Mohamed, Krishnaswamy Panchanatheswaran, J.N. Low, Christopher Glidewell

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Abstract

The title compound is a co-crystal of [2-[(benzoylmethylene)diphenyl-lambda5-phosphino]ethyl]diphenylphosphine oxide, [2-[(benzoylmethylene)diphenyl-lambda5-phosphino]ethyl]diphenylphosphine and water in an approximate 2:1:3 ratio, with an overall composition of C34H30O1.678P2.H2O. The ylidic portion shows the expected electronic polarization, and the organic components are linked by a combination of C-H...O and C-H...pi(arene) hydrogen bonds.

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The title compound is a co-crystal of [2-[(benzoylmethylene)diphenyl-lambda5-phosphino]ethyl]diphenylphosphine oxide, [2-[(benzoylmethylene)diphenyl-lambda5-phosphino]ethyl]diphenylphosphine and water in an approximate 2:1:3 ratio, with an overall composition of C34H30O1.678P2.H2O. The ylidic portion shows the expected electronic polarization, and the organic components are linked by a combination of C-H...O and C-H...pi(arene) hydrogen bonds.

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Available abstract

The title compound is a co-crystal of [2-[(benzoylmethylene)diphenyl-lambda5-phosphino]ethyl]diphenylphosphine oxide, [2-[(benzoylmethylene)diphenyl-lambda5-phosphino]ethyl]diphenylphosphine and water in an approximate 2:1:3 ratio, with an overall composition of C34H30O1.678P2.H2O. The ylidic portion shows the expected electronic polarization, and the organic components are linked by a combination of C-H...O and C-H...pi(arene) hydrogen bonds.

Key concepts: Diphenylphosphine, Diphenylphosphine oxide, Chemistry, Crystal structure, Hydrogen bond, Medicinal chemistry, Crystallography, Organic chemistry

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